Practical Chemistry

Growing crystals


Apparatus needed:

  • Test tube
  • Stirring rod (long)
  • Water bath setup (400cm3 beaker, tripod, gauze and bunsen burner)
  • Spatula
  • Microscope and slide

Chemicals:

  • Potassium aluminium sulphate
  • Sodium chloride
  • Potassium nitrate
  • Copper sulphate
  • Chromium aluminium sulphate

Instructions:

  1. Set up a water bath using a 400 cm3 beaker half full of water.
  2. Measure out 5cm3 of water into a clean test tube and place the test tube in the water bath to warm up..
  3. Add a spatula of the solute to be crystallised and if it all dissolves (with careful stirring) add more solute until some remains undissolved at the bottom of the test tube.
  4. Allow any undissolved solid to settle at the bottom of the tube and withdraw a smal quantity of the solution using a dropping pipette.
  5. Place one drop of the solution on a microscope slide and watch for crystal formation through the microscope lens.
  6. Draw the shape of the crystal produced.

Write up:

Aim:   What do you hope to find out
Hypothesis:   Not needed in this case
Method:   Refer to the instructions and include any changes you had to make
Diagram:   Show any assembled apparatus or complex operations carried out.
Results:   Tabulated if possible
Conclusions:   How can you explain your results
Evaluation:   Do you think that the experiment is adequate for the aim? Can it be improved? What would you do if you were to do it again?

 


 
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Copyright: 2003 Isis Publication